Analysis of deoxynivalenol and its derivatives (batch and single dernel) using gas chromatography mass spectrometry.
MIROCHA, C.J., KOLACZKOWSKI,E., XIE, W.P., YU,H, and JELEN, H.
Jounal of Agricultural and Food Chemistry 46: 1414 – 1418.
1998
บทคัดย่อ
A method is described for the analysis of DON and its derivatives in wheat and barley using combination GC/MS. The method has been designed for the analysis of large batch (100 g) samples and single kernels. The sensitivity of the method is 50mg/kg and the recovery for 1, 5 and 10 mg/kg from wheat is 97, 88 and 88% respectively. A comparison of methods was made between two laboratories using GC/EC and this method and there was no significant difference between the results of the two methods. The method is also applicable to 15 – acetyIDON and NIV.