Solid-phase extraction method for patulin in apple juice and unfiltered apple juice.
TRUCKSESS, M.W. and TANG, Y.F.
Journal of AOAC International 82 : 1109-1113.
1999
บทคัดย่อ
A soild-phase extraction method is described for the determination of patulin in apple juice and unfiltered apple juice. A portion of the test sample was passed through a macroporous copolymer cartridge and was washed with 1% sodium bicarbonate and then with 1% acetic acid. Patulin was eluted with 2% acetonitrile in anhydrous ethyl ether and was determined by reversed phase LC with UV detection. Recoveries ranged from 93 to 104% in test samples spiked at 20 – 100 mg/L.