Sample preparation and high – resolution separation of mycotoxins possessing carboxyl groups.
WILKES, J.G. and SUTHERLAND, J.B.
Jornal of Chrmatography B 717: 135 – 156.
1998
บทคัดย่อ
This review with 104 references discusses the difficulties involved in the chromatographic analysis of carboxyl – containing mycotoxins, such as fumonisin B1, OA and citrinin. Fluorescence derivatisation and electrospray LC – MS have now made it possible to detect trace levels of mycotoxins. The purity of mycotoxin standards for toxicological studies can be determined by LC with either an evaporative light scattering detector or electrospray MS. New develpments in capillary electrophoresis, nonporous microspere LC and detection methods for low volatility compounds show promise for improving the analysis of mycotoxins in the future.