Determination of the mycotoxin moniliformin in cereals by high-performance liquid chromatography and fluorescence detection.
FILEK, G. and LINDNER, W.
Journal of Chromatography A 732 : 291-298.
1996
บทคัดย่อ
The development of a selective and sensitive HPLC fluorescence assay for the determination of moniliformin in plant extracts is described. By introducing a derivatisation reaction with 1,2-diamino-4,5-dichlorobenzene the overall determination sensitivity and the chromatographic selectivity on a reverse phase HPLC system are increased. Fluorescence detection enabled the reduction of the determination limit of moniliformin from 0.05 (UV detection) to 0.02mg/kg maize.